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state of iodine. what is the oxidation state of iodine in the product?


Reaction under Andrews’ conditions
In the next titration you will see that the same oxidant, IO3-, and reductant, I-, can undergo a different reaction by altering the conditions. The reaction will again be done in acidic solution, but this time will contain a large concentration of Cl- (obtained by adding concentrated hydrochloric acid to the reaction vessel). This titration will also illustrate yet another visual means of detecting the end-point.

Weigh accurately about 2.0 g of potassium iodide and make it up to 250 ml of aqueous solution in a volumetric flask. Transfer 25 ml of this solution by pipette to a 250 ml stoppered bottle, then add 25 ml of water, 60 ml concentrated hydrochloric acid (CARE – CORROSIVE - do this procedure at the sink), and about 5 ml of CH2Cl2 (TAKE CARE - do this procedure in the fume hood). Cool the bottle to room temperature, then add, from a burette, a standard 0.

2007-03-24 06:01:40 · 1 answers · asked by cat_ren_03 1 in Science & Mathematics Chemistry

1 answers

I'm willing to bet that you saw a purple colour in the organic solvent at the end.
That would have been I2, oxidation state zero.

2007-03-24 21:52:29 · answer #1 · answered by Gervald F 7 · 0 0

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