how to prepare a dry sample of aspirin from a solution of aspirin?

Answer 1

Many commercial solutions of aspirin contain additional compounds which make a simple "let it evaporate" not possible.

If the purpose of wanting a solid is to measure the yield from a reaction or in order to measure a melting point, then what you need to do is crystallize (or recrystallize) the aspirin.

If what you have is an aqueous solution, make sure that it is basic (not acidic) and the extract with dichloromethane or diethyl ether. The CH2Cl2 or ether solution can then be dried with sodium or magnesium sulfate to remove the water. Upon evaporation, you will get solid aspirin.

This solid could be redissolved and allowed to form crystals if a very pure aspirin is needed.

Answer 2

Pour it into a mold and allow it to dry. For example, do you have any plastic packaging for allergy or other medicine that requires that you push out the tab? You may be able to use that as a mold. I don't know if you'll need to add a small amount of parafin so the dry powder holds together.


... just my suggestion.

Answer 3

What am i able to declare. i develop into youthful while that was once the norm. They used to declare that delivery administration meds weren't needed if the aspiring between the knees develop into there in any respect circumstances without falling. i do no longer understand if there is human beings here that keep in mind this word: "Her rabbit died as a results of fact she enable the aspirin fall from between her knees". It develop right into a sarcastic thank you to declare that the girl develop into no longer a "stable female". It develop into an insult despite if it develop into the norm. Republicans, decide to deliver back that ideas-set. those regulations stored the ladies of that evaluate their place, so so which you may talk. non secular women do no longer ought to apply delivery administration, yet coverage companies could desire to cover for people who're no longer non secular and who decide to apply their unfastened will how ever they want. Religions are actually not being mandated to do yet EMPLOYERS ARE. If a church CHOOSES TO BE AN corporation, IT could desire to ABIDE by way of WHAT EMPLOYERS ARE MANDATED TO ABIDE. this does not take place in the international places the place coverage isn't an corporation's duty. different than that over here all workers are required to pay a minimum of three quarters of their coverage top rate. If a female is procuring a minimum of three quarters of her coverage then the coverage companies are meant to cover for delivery administration. the only way they do no longer look to be assume to pay for it somewhat is that if those meds could be bought OTC. i could propose that churches end being for earnings and require that individuals volunteer in that way they do no longer look to be employers. unfastened will is unfastened will. And in ordinary terms God is the choose of all. churches ought to stick to what Jesus pronounced.

Answer 4

distillation.....